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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 843896Generated: October 31, 2026

Methyl isothiocyanate → HCID 54517905, compound

https://huagongshe.com/reaction/843896

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl isothiocyanateHCID 11167—
Reactant6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazoleHCID 22611560—
SolventDichloromethaneHCID 6344—
ProductHCID 54517905HCID 5451790548%

Reaction Steps

To a solution of 10.0 mg (0.0437 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole in 3.0 mL dichloromethane were added 6.2 mg (0.0874 mMol) methyl isothiocyanate. The reaction was mixed for 48 hours and to it were then added 0.15 gm (0.0874 mMol) aminomethylated polystyrene and the reaction mixed for an additional 18 hours. The reaction mixture was then filtered and the volatiles evaporated to give 6.3 mg (48%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06380201B1
Source datasetuspto-grants-2002_04
ORD IDord-26d1f679c886472b935029df225cddc4
Source noteuspto-grants-2002_04