HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22613081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86758010 | HCID 86758010 | — |
| Solvent | DCM MeOH AcOH | HCID 21877243 | — |
| Product | HCID 22613081 | HCID 22613081 | — |
Reaction Steps
In a manner similar to example AIV-2-1, 2,4-dioxo-4-(3-phenylsulfanyl-phenyl)-butyric acid ethyl ester was formed and the crude material was hydrolyzed in a manner similar to example AIV-3-1 using 1N NaOH to afford L-1 as a yellow solid. Rf=0.32 (6:6:94 MeOH/AcOH/CH2Cl2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380249B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-666ee53fd5c845fd8ecab7befba5d744 |
| Source note | uspto-grants-2002_04 |