HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexen-1-one, 4,4-dimethyl- | HCID 136839 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Cyclohexanone, 4,4-dimethyl- | HCID 138166 | 92.5% |
Reaction Steps
6.7 g of 4,4-dimethyl-2-cyclohexen-1-one and 2 g of 10% Pd/C are added to 65 ml of EtOAc and the mixture is hydrogenated at RT under atmospheric pressure until the theoretical volume of hydrogen has been absorbed. The catalyst is filtered off and the filtrate is then concentrated to give 6.3 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380230B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-39b1a2aaa52348eaa50e809193d2df41 |
| Source note | uspto-grants-2002_04 |