Chlorosuccinimide → HCID 14155403, compound

HRID 844987Notes

Reaction equation

HRID 844987 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][C:11]=1[Cl:12])[C:5]([O:7][CH3:8])=[O:6].[Cl:13]N1C(=O)CCC1=O>>[NH2:1][C:2]1[C:3]([Cl:13])=[C:4]([CH:9]=[CH:10][C:11]=1[Cl:12])[C:5]([O:7][CH3:8])=[O:6]

Participants

3

Reactant 2

HCID 31398ChlorosuccinimideHCID 593055Methyl 3-Amino-4-chlorobenzoate

Product 1

HCID 14155403HCID 14155403, compound

Procedure

This material was prepared by chlorination of methyl 3-amino-4-chlorobenzoate with N-chlorosuccinimide. The product was isolated as a solid, m.p. 50°-52° C. The product was characterized by IR and 1H NMR spectroscopy and combustion analysis.

Workup

  1. customThe product was isolated as a solid, m.p. 50°-52° C

Sources & evidence

ORD record
ord-bc189d24b0c2436f8d20b4bd1df4d500
Source dataset
uspto-grants-1988_07
Patent number
US04755212

Reaction notes

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