Chlorosuccinimide → HCID 15017527, compound

HRID 844990Notes

Reaction equation

HRID 844990 reaction equation
[Br:1][C:2]1[C:8]([Cl:9])=[CH:7][C:5]([NH2:6])=[C:4]([CH3:10])[CH:3]=1.[Cl:11]N1C(=O)CCC1=O>>[Br:1][C:2]1[CH:3]=[C:4]([CH3:10])[C:5]([NH2:6])=[C:7]([Cl:11])[C:8]=1[Cl:9]

Participants

3

Reactant 2

HCID 31398ChlorosuccinimideHCID 71720264-bromo-5-chloro-2-methylaniline

Product 1

HCID 15017527HCID 15017527, compound

Procedure

This material was prepared from 4-bromo-5-chloro-2-methyl aniline by chlorination with N-chlorosuccinimide. The product was isolated as a solid, m.p. 66°-68° C. The product was characterized by IR and 1H NMR spectroscopy and combustion analysis.

Workup

  1. customThe product was isolated as a solid, m.p. 66°-68° C

Sources & evidence

ORD record
ord-444a973a7a874193b06b4383f7bad168
Source dataset
uspto-grants-1988_07
Patent number
US04755212

Reaction notes

Loading…