HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14154537, compound → HCID 14154538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14154537 | HCID 14154537 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14154538 | HCID 14154538 | 95.9% |
Reaction Steps
0.35 g 1,3-Dipropyl-8-(2-furanyl)xanthine is dissolved in 50 ml methanol, to which is added 0.5 g Raney nickel and the mixture reduced under a hydrogen atmosphere of 200 psi at 100° C. The mixture is then filtered, the filtrate concentrated to yield 0.34 g of the 1,3-dipropyl-8-(2-tetrahydrofuranyl)xanthine as a white solid, mp 155°-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04755517 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-8d9c39d7deac43f68cf754ec221b64b4 |
| Source note | uspto-grants-1988_07 |