Hydrochloric Acid → HCID 20133501, compound

Participants

Reaction Steps

Over 1 hour 30 min. a solution of 60.5 g (0.232 mole) of stannic chloride in 75 ml of benzene is poured into a solution maintained at about 5° C. of 33.6 g (0.200 mole) of 1,3,5-trimethoxybenzene and of 30.5 g (0.216 mole) of 4-chlorobutyryl chloride in 150 ml of benzene, with agitation for 3 hours at ambient temperature. The reactional medium is poured on to 250 ml of iced 4N hydrochloric acid and the organic phase is decanted.

Provenance & Evidence