HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Mercaptopropionic Acid → HCID 14011802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Mercaptopropionic Acid | HCID 6514 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 14011802 | HCID 14011802 | — |
Reaction Steps
The title compound was prepared according to the method of Example 5 from 3-mercaptopropionic acid (6.1 g, 0.057 mole); sodium (3.9 g, 0.17 mole); 1-bromo-2-chloroethane (12.4 g, 0.086 mole); and 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (13.7 g, 0.057 mole), purified by chromatography on silica and recrystallized from ethyl acetate/hexane, m.p. ca. 57.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04755524 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-f7baf4ae14754803b6d2eb5e92d16eeb |
| Source note | uspto-grants-1988_07 |