HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 20133512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 20133523 | HCID 20133523 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20133512 | HCID 20133512 | — |
Reaction Steps
Oxalyl chloride (3 ml) was added to a solution of the compound of Example 41 (2.3 g) in benzene (50 ml) and stirred for 3 hours at room temperature. The reaction volume was reduced and methyl alcohol (100 ml) added. After evaporation of the solvents, the product (an oil) was purified by chromatography on silica.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04755524 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-5c82a2630ccd4c38b5443081cf763bbb |
| Source note | uspto-grants-1988_07 |