HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14208607, compound → HCID 14208608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14208607 | HCID 14208607 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 14208608 | HCID 14208608 | 58.1% |
Reaction Steps
A solution of the product from Example 1 (6.0 g, 0.0192 mole) in trifluoroacetic acid (20 mL) was stirred at room temperature overnight, was stripped to an oil, and crystallized with ethyl acetate/ether to yield 2.87 g solid, m.p. 140°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04756742 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-85db777048854489b51f7a2015fb3f38 |
| Source note | uspto-grants-1988_07 |