HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Isoleucine, methyl ester → HCID 131715626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Isoleucine, methyl ester | HCID 75735 | — |
| Reactant | HCID 131715627 | HCID 131715627 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131715626 | HCID 131715626 | — |
Reaction Steps
The L-isoleucine, methyl ester, isomer A product from part (a) (0.25 g., 0.544 mmole) is dissolved in a solution of hydrochloric acid in dioxane (2N, 2.25 ml.). After keeping the solution at room temperature for 4 hours, it is evaporated in vacuo to give N-[[[(3S)-3-amino-2-hydroxy-5-methylhexyl](1-methylethyl)amino]carbonyl]-L-isoleucine, methyl ester, isomer A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04757050 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-dd03c7b0a59c492ebf4c8b8ba692616d |
| Source note | uspto-grants-1988_07 |