HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131715628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | L-Isoleucine, methyl ester | HCID 75735 | — |
| Reactant | HCID 131715630 | HCID 131715630 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131715628 | HCID 131715628 | — |
Reaction Steps
The isoleucine, methyl ester product from part (d) (0.43 g., 1.03 mmole) is dissolved in a solution of hydrochloric acid in dioxane (2N, 3 ml.) and kept at room temperature for 2.5 hours. The mixture is then concentrated to dryness in vacuo to give N-[[[(3S)-3-amino-2-hydroxy-5-methylhexyl]amino]carbonyl]-L-isoleucine, methyl ester, monohydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04757050 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-8d8d4beb60bd4bd3b2a1b8f7e712cdbc |
| Source note | uspto-grants-1988_07 |