HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 70407477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 54319701 | HCID 54319701 | — |
| Product | HCID 70407477 | HCID 70407477 | — |
Reaction Steps
Under nitrogen, a solution of 0.19 g of 9-acetyl-5-bromoethyl-beta-carboline-3-carboxylic acid ethyl ester in 5 ml of ethanol is mixed with 1 ml of morpholine and stirred overnight at room temperature. After addition of water the crystallizate is suctioned off and recrystallized from ethanol/diethylether. 0.11 g (64%) is obtained. Melting point 285° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04757070 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-e92373eca9bc45ba85c0ed93dea926fe |
| Source note | uspto-grants-1988_07 |