HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 70407125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 70407076 | HCID 70407076 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70407125 | HCID 70407125 | — |
Reaction Steps
A suspension of 0.11 g of 9-acetyl-5-(1-imidazolylmethyl)-beta-carboline-3-carboxylic acid ethyl ester in 5 ml of ethanol is mixed with 10 mg of K2CO3 and refluxed for two hours. After filtering, the solution is concentrated in a vacuum, the residue is mixed with water, suctioned off and recrystallized from water. Yield 70 mg (71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04757070 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-02ec03d702b54b4892f0322210ae0531 |
| Source note | uspto-grants-1988_07 |