Hydrazine hydrate (1:1) → HCID 14011678, compound

HRID 845260Notes

Reaction equation

HRID 845260 reaction equation
[CH3:1][C:2]1[NH:3][C:4]([CH3:40])=[C:5]([C:24]([O:26][CH2:27][CH2:28][N:29]2C(=O)C3=CC=CC=C3C2=O)=[O:25])[CH:6]([C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([N+:21]([O-:23])=[O:22])[CH:16]=2)[C:7]=1[C:8]([O:10][CH2:11][CH2:12][O:13][CH3:14])=[O:9].O.NN>>[CH3:1][C:2]1[NH:3][C:4]([CH3:40])=[C:5]([C:24]([O:26][CH2:27][CH2:28][NH2:29])=[O:25])[CH:6]([C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([N+:21]([O-:23])=[O:22])[CH:16]=2)[C:7]=1[C:8]([O:10][CH2:11][CH2:12][O:13][CH3:14])=[O:9]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 14011673HCID 14011673, compound

Product 1

HCID 14011678HCID 14011678, compound

Procedure

Prepared by a method analogous to that of Example 1(b) from 10.0 g (18.2 mmol) of 1,4-dihydro-2,6-dimethyl-3-(2-methoxyethoxy)carbonyl-4-(3-nitrophenyl)-5-(2-phthalimidoethoxy)carbonyl-pyridine and 2.65 ml (54.6 mmol) of hydrazine hydrate.

Sources & evidence

ORD record
ord-80dae987f5354f7881090ac36db16fab
Source dataset
uspto-grants-1988_07
Patent number
US04757080

Reaction notes

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