HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20132514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 14011674 | HCID 14011674 | — |
| Product | HCID 20132514 | HCID 20132514 | 96.5% |
Reaction Steps
Prepared by a method analogous to that of Example 1(b) from 10.94 g (20 mmol) of 1,4-dihydro-2,6-dimethyl-3-isobutoxycarbonyl-4-(2-nitrophenyl)-5-(2-phthalimidoethoxycarbonyl)-pyridine and 3.0 ml (60 mmol) of hydrazine hydrate. 8.06 g (96%) of a viscous yellow oil are obtained. This product is used for reactions without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04757080 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-65b79e3f06fd416da97dd6def90503e0 |
| Source note | uspto-grants-1988_07 |