Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 2-((3-nitrophenyl)methylene)-3-oxobutanoate → 1,4-Dihydro-2,6-dimethyl-3-methoxycarbonyl-4-(3-nitrophenyl)-5-(11-phthalimido-undecyloxy)carbonyl-pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 2-((3-nitrophenyl)methylene)-3-oxobutanoate | HCID 1536427 | — |
| 반응물 | 3-Amino-crotonic acid-(11-phthalimido-undecyl)ester | HCID 67903688 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1,4-Dihydro-2,6-dimethyl-3-methoxycarbonyl-4-(3-nitrophenyl)-5-(11-phthalimido-undecyloxy)carbonyl-pyridine | HCID 20132490 | 98% |
반응 단계
Prepared by a method analogous to that of Example 1(a) from 9.33 g (37.5 mmol) of 2-(3-nitrobenzylidene)-acetoacetic acid methyl ester and 15.00 g (37.5 mmol) of 3-amino-crotonic acid-(11-phthalimido-undecyl)ester. 23.18 g (98%) of yellow crystals, melting point 130°-132° C., obtained from methanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04757080 |
| 출처 데이터셋 | uspto-grants-1988_07 |
| ORD ID | ord-61e341e2281a457cb5d5ada6e4335639 |
| 출처 메모 | uspto-grants-1988_07 |