Formaldehyde → HCID 20132563, compound

HRID 845281Notes

Reaction equation

HRID 845281 reaction equation
[CH2:1]([N:8]([CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[OH:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:17]=O.[CH2:19]([NH:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>>[CH2:10]([N:8]([CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[O:9][CH2:17][N:25]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 3

HCID 712FormaldehydeHCID 8920DihexylamineHCID 69297Dibenzylhydroxylamine

Product 1

HCID 20132563HCID 20132563, compound

Procedure

The procedure of Example I is repeated using 21.33 g of dibenzylhydroxylamine, 9.73 g of aqueous formaldehyde (37%) solution and 18.54 g of di-n-hexylamine, to afford the title compound.

Sources & evidence

ORD record
ord-27f42d2e5cfa4dd3baab52956a652991
Source dataset
uspto-grants-1988_07
Patent number
US04757102

Reaction notes

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