Formaldehyde → HCID 20132573, compound

HRID 845285Notes

Reaction equation

HRID 845285 reaction equation
[CH2:1]([N:8]([CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[OH:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:17]=O.[C:19]1([NH:25][C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:10]([N:8]([CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[O:9][CH2:17][N:25]([C:19]1[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1)[C:26]1[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 3

HCID 712FormaldehydeHCID 11487DiphenylamineHCID 69297Dibenzylhydroxylamine

Product 1

HCID 20132573HCID 20132573, compound

Procedure

The procedure of Example I s repeated using 21.33 g of dibenzylhydroxylamine, 9.46 g of aqueous formaldehyde (37%) solution and 16.92 g of diphenylamine, to afford the title compound as a colorless liquid with a mass spectrum, NMR and IR consistent with the desired structure.

Sources & evidence

ORD record
ord-15c3efa6a02a456793ab7307d15abe93
Source dataset
uspto-grants-1988_07
Patent number
US04757102

Reaction notes

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