HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 14157411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 1-Chloro-4-(4-methylpent-1-en-3-yl)benzene | HCID 13616547 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14157411 | HCID 14157411 | — |
Reaction Steps
A mixture of 4 g of the product of Example 1 and 4.5 g of m-chloroperbenzoic acid in 50 mL of chloroform was stirred overnight at room temperature and filtered. The filtrate was washed with aqueous NaHSO3, aqueous NaHCO3, brine, dried (Na2SO4), and concentrated. The residue was a mixture of diastereomeric epoxides.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04758262 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-3820bf2cf01a4547b708180a0fa88169 |
| Source note | uspto-grants-1988_07 |