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HRID84540

反应详情

EQUATION

反应方程式

HRID 84540 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCN
HCID66053

N,N-Dimethylethylenediamine

C4H12N2

结构：CN(C(=O)c1cc2c(s1)-c1ccccc1OCC2)c1ccc(C(=O)O)cc1Cl
HCID66868923

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCNC(=O)c1ccc(N(C)C(=O)c2cc3c(s2)-c2ccccc2OCC3)c(Cl)c1
HCID57900144

未命名化合物

PROCEDURE

实验过程

3-Chloro-4-(N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamido)benzoic acid and N1,N1-dimethylethane-1,2-diamine were reacted by a procedure similar to that to prepare 137 in Example 47 to give 248. MS: (ESI+) 484.3

WORKUP

后处理

  1. customthat to prepare 137 in Example 47