HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentane → HCID 136342795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentane | HCID 8003 | — |
| Reactant | Trimethylorthoacetate | HCID 21927715 | — |
| Reactant | HCID 135603722 | HCID 135603722 | — |
| Product | HCID 136342795 | HCID 136342795 | — |
Reaction Steps
A mixture of 3.0 g of 3-(4-hydroxyphenyl)-1,2,4-thiadiazole-5-sulfonamide and 20 ml of trimethylorthoacetate was stirred at room temperature for 42 hours. Pentane (25 ml) was added and stirring continued overnight. The precipitated solid was triturated with benzene and collected to give 2.4 g of powder, m.p. 190°-192°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04758578 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-bcaef99a04f14710ab321dd85423008e |
| Source note | uspto-grants-1988_07 |