HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 86742271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 86742267 | HCID 86742267 | — |
| Reactant | HCID 86742272 | HCID 86742272 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86742271 | HCID 86742271 | — |
Reaction Steps
A solution of cis-octahydro-2-oxo-1H-indole-1acetic acid ethyl ester (15.43 g, 0.068 mole) in methanol (200 ml) is saturated with ammonia and stirred at ambient temperatures 24 hours. The solution is concentrated at reduced pressure to yield a solid. cis-Hexahydro-2-oxo-cyclopenta[b]pyrrole-1(2H)-acetamide with a mp 145°-145.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04758585 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-575be8da29294df2b3db027c8f16a8d2 |
| Source note | uspto-grants-1988_07 |