HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 14182978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 70406985 | HCID 70406985 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14182978 | HCID 14182978 | — |
Reaction Steps
A solution of trans-octahydro-2-oxo-1H-indole-1-acetic acid ethyl ester; (7.7 g, 0.032 mole) in methanol (200 ml) in methanol (200 ml) is saturated with ammonia and stirred at ambient temperatures 24 hours. The solution is concentrated at reduced pressure to yield a solid, trans-hexahydro-2-oxocyclohexa[b]pyrrol-1-(2H)-acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04758585 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-71853acb481a48cf80a1471e3910314b |
| Source note | uspto-grants-1988_07 |