HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54180226, compound → HCID 53769050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54180226 | HCID 54180226 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 53769050 | HCID 53769050 | — |
Reaction Steps
In a manner similar to Example 2, 1.8 g (5 mmol) of ethyl 5-(1-benzylindol-3-yl)-2-ethyl-2,4-pentadienoic acid was hydrolyzed to give the corresponding acid, m.p. (ether): 169-170. NMR (CDCl3 /DMSO-d6) spectrum shows broad triplet and quartet at δ1.10 and δ2.47 respectively; the benzyl methylene signal appears at δ5.30 as a broad singlet.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04758586 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-bf067b3334024174a0ec67ef6a100734 |
| Source note | uspto-grants-1988_07 |