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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 845940Generated: October 30, 2026

Dimethyl Sulfate → HCID 20130648, compound

https://huagongshe.com/reaction/845940

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfateHCID 6497—
ReactantHCID 20130578HCID 20130578—
SolventDimethylformamideHCID 6228—
ProductHCID 20130648HCID 20130648—

Reaction Steps

using isopropyl 2-chloro-4-fluoro-5-[5-cyano-3,6-dihydro-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate and dimethyl sulphate in dimethylformamide there is obtained isopropyl 2-chloro-4-fluoro-5-[5-cyano-3,6-dihydro-3-methyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate, 1H--NMR (CDCl3, 400 MHz) 8.00 ppm (s, 1H), 7.83 ppm (d, 1H), 7.38 ppm (d, 1H), 5.25 ppm (m, 1H), 3.55 ppm (s, 3H), 1.37 ppm (2xd, 6H),

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04760163
Source datasetuspto-grants-1988_07
ORD IDord-52de0326156c4eb287ff4cbc3498c753
Source noteuspto-grants-1988_07