HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylamine → HCID 18625054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | (2,6-Dinitrophenyl)methanol | HCID 119332 | — |
| Reactant | 4-(Trifluoromethyl)benzenesulfonyl chloride | HCID 2777399 | — |
| Product | HCID 18625054 | HCID 18625054 | 38% |
Reaction Steps
The procedure of Example 11 was employed except that the reagents were 2.00 g of 2,6-dinitrobenzyl alcohol, 2.71 g of 4-(trifluoromethyl)benzenesulfonyl chloride and 2.2 mL of dicylohexylamine. The crude product was recrystallized using carbon tetrachloride/chloroform to give 1.55 g (38% yield) of white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05135838 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-c08db09b04ad401f89341f5e36a4cbbf |
| Source note | uspto-grants-1992_08 |