HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 14698596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 2-(4-Aminophenyl)-2-methylpropanenitrile | HCID 10057801 | — |
| Product | HCID 14698596 | HCID 14698596 | 85% |
Reaction Steps
Analogously to Example 25, 4-(1-cyano-1-methylethyl)-aniline is reacted with 4-methoxybenzoic acid chloride to give a yield of 85% of theory of the title compound in the form of beige crystals; m.p. 169°-171° C. A sample thereof is recrystallised from ethanol and then has a melting point of 172°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05135949 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-9d60ed0b4bee4089b1642f04d135403d |
| Source note | uspto-grants-1992_08 |