HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 888434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14698592 | HCID 14698592 | — |
| Product | HCID 888434 | HCID 888434 | — |
Reaction Steps
2.0 g. 4-(1,1-Dimethylethyl)-N-[4-(ethoxycarbonylmethoxy)-phenyl]-benzamide (Example 31) are heated in 20 ml. 2N aqueous sodium hydroxide solution, then acidified with concentrated hydrochloric acid, filtered off with suction and washed with water. After recrystallisation from ethyl acetate, there is obtained 1.2 g. (65% of theory) of the title compound; m.p. 179°-181° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05135949 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-7a544cf21af2493fbe2aa877bb2b26c5 |
| Source note | uspto-grants-1992_08 |