反应详情

Piperidine, 1.2 ml, was added to a boiling solution of 3-nitrobenzalacetophenone (10 g, 0.04 mole) and 3-methoxybenzenethiol (6.64 g, 0.048 mole) in 100 ml benzene . After standing for 30 minutes without further heating, acetic acid, 10 ml, was added. The solution then was poured into water (about 100 ml), extracted with methylene chloride (5×100 ml), washed with water, dried (Na2SO4) and evaporated to dryness to yield the title compound as a solid, mp 105°.

1. additionwas added
2. extractionextracted with methylene chloride (5×100 ml)
3. washwashed with water
4. dry with materialdried (Na2SO4)
5. customevaporated to dryness