HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 13693406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13693403 | HCID 13693403 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13693406 | HCID 13693406 | — |
Reaction Steps
The ester from Step B (1.07 g) was saponified with 1N NaOH (5 ml) and methanol (5 ml) and THF (5 ml) to provide after acidification, extraction into CH and evaporation to dryness the title compound, mp 69°-71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05135940 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-6efb5349747849ec9cd47f01c1840f87 |
| Source note | uspto-grants-1992_08 |