HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphosgene → HCID 19882834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphosgene | HCID 10426 | — |
| Reactant | 2,4-Dichloro-5-methylaniline | HCID 283314 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19882834 | HCID 19882834 | 107.9% |
Reaction Steps
In a manner similar to Kurita, et al., J. Org. Chem., 41, 2070 (1976), incorporated herein by reference, the reaction of 3.43 g (0.0156 mole) of 2,4-dichloro-5-methylaniline and 3.5 g (0.018 mole) of trichloromethyl chloroformate in 50 mL of toluene produced 3.4 g of 2,4-dichloro-5-methylphenyl isocyanate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05136868 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-91b1f67804804a0f8d454bc9684c7386 |
| Source note | uspto-grants-1992_08 |