HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azidotrimethylsilane → HCID 136041366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azidotrimethylsilane | HCID 78378 | — |
| Reactant | HCID 19882834 | HCID 19882834 | — |
| Product | HCID 136041366 | HCID 136041366 | 27.3% |
Reaction Steps
In the manner of Example 1, Step A, the reaction of 3.4 g (0.016 mole) of 2,4-dichloro-5-methylphenyl isocyanate and 3.6 g (0.031 mole) of trimethylsilyl azide produced 1.07 g of 1-(2,4-dichloro-5-methylphenyl)-1,4-dihydro-5H-tetrazol-5-one as a solid, mp 135°-137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05136868 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-a799c848cea942e9b52542c03f4e06bf |
| Source note | uspto-grants-1992_08 |