HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2,4-Dichloro-5-methoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-(2,4-Dichloro-5-methoxyphenyl)acetamide | HCID 14593783 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,4-Dichloro-5-methoxyaniline | HCID 1476636 | 54.3% |
Reaction Steps
In the manner of Example 2, Step C, the reaction of 37.4 g (0.16 mole) of 2,4-dichloro-5-methoxyacetanilide with 12.8 g (0.32 mole) of sodium hydroxide in 30 mL of water and 30 mL of ethanol produced 16.7 g of 2,4-dichloro-5-methoxyaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05136868 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-b63b709da36d4403aeed1e3a384f5dcc |
| Source note | uspto-grants-1992_08 |