HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloro-2-propanol → 1,3-Bis[(2-hydroxyethyl)phenylamino]-2-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloro-2-propanol | HCID 7289 | — |
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | N-(2-Hydroxyethyl)aniline | HCID 31235 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1,3-Bis[(2-hydroxyethyl)phenylamino]-2-propanol | HCID 15926186 | — |
Reaction Steps
The mixture consisting of 2 moles (274.4 g) of N-β-hydroxyethylaniline, 140 g of calcium carbonate and 1.2 moles (154.8 g) of 1,3-dichloro-2-propanol in 1 liter of water is heated for 6 hours under water reflux.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137538 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-c963fcf93c1c49f8911e1659edd05143 |
| Source note | uspto-grants-1992_08 |