HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19883104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 19883096 | HCID 19883096 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19883104 | HCID 19883104 | — |
Reaction Steps
A solution of the pyridone prepared in stage (v) (0.27 g) in dichoromethane (30 cm3) under nitrogen was cooled to 0° C. and a solution of mesyl chloride in chloroform was added (0.12 g in 5 cm3). The reaction mixture was stirred for 5 minutes then treated with triethylamine (0.1 g) in dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137886 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-2eb8ac82c7904b64b2d7c744f74dc0f9 |
| Source note | uspto-grants-1992_08 |