HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 19883106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 19883110 | HCID 19883110 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 19883106 | HCID 19883106 | — |
Reaction Steps
To a stirred solution of 2-(pyrrole-1-sulphonyl)pyrid-6-one (0.22 g) in dichloromethane (20 cm3) under nitrogen at 0° C. was added in solution of mesyl chloride (0.124 g) in dichloromethane (5 cm3) and triethylamine (0.109 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137886 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-52f716cdf9d04c7fa2be3b267c9afd4d |
| Source note | uspto-grants-1992_08 |