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HRID846590

反应详情

EQUATION

反应方程式

HRID 846590 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Cl
HCID31297

Methanesulfonyl chloride

CH3ClO2S

结构：O=c1cccc(S(=O)(=O)n2cccc2)[nH]1
HCID19883110

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)Oc1cccc(S(=O)(=O)n2cccc2)n1
HCID19883106

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

To a stirred solution of 2-(pyrrole-1-sulphonyl)pyrid-6-one (0.22 g) in dichloromethane (20 cm3) under nitrogen at 0° C. was added in solution of mesyl chloride (0.124 g) in dichloromethane (5 cm3) and triethylamine (0.109 g).