Methanol → HCID 14988335, compound

HRID 846628Notes

Reaction equation

HRID 846628 reaction equation
C([O:4][CH2:5]/[CH:6]=[CH:7]\[C:8]1[CH:13]=[CH:12][C:11]([O:14][CH:15]([O:17][CH2:18][CH3:19])[CH3:16])=[CH:10][CH:9]=1)(=O)C.CO.C(=O)([O-])[O-].[K+].[K+]>O>[CH2:18]([O:17][CH:15]([O:14][C:11]1[CH:10]=[CH:9][C:8](/[CH:7]=[CH:6]\[CH2:5][OH:4])=[CH:13][CH:12]=1)[CH3:16])[CH3:19]

Participants

5

Reactant 3

HCID 887MethanolHCID 11430Potassium CarbonateHCID 14988334HCID 14988334, compound

Product 1

HCID 14988335HCID 14988335, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

7.8 Grams of 4(Z)-(1-ethoxyethoxy)cinnamyl acetate and 50 ml of methanol solution containing 5 g of potassium carbonate were stirred at a room temperature for 2 hours. The solvent was removed by evaporation, and to the residue thus obtained was added water and extracted with ether. The ether extract was washed with water, dried and the solvent remove by evaporation to yield 4(Z)-(1-ethoxyethoxy)cinnamyl alcohol.

Workup

  1. customThe solvent was removed by evaporation
  2. customto the residue thus obtained
  3. extractionextracted with ether
  4. extractionThe ether extract
  5. washwas washed with water
  6. customdried
  7. customthe solvent remove by evaporation

Sources & evidence

ORD record
ord-0e6bac46c37f40da975c2ff3cd62a836
Source dataset
uspto-grants-1992_08
Patent number
US05137889

Reaction notes

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