HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67915154, compound → HCID 19883665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67915154 | HCID 67915154 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19883665 | HCID 19883665 | 95.9% |
Reaction Steps
0.88 g of methyl 4-[(Z)-7-(dimethylamino)-1-heptenyl]benzoate was dissolved in 20 ml of ethanol, 20 mg of 5 percent palladium on carbon were added thereto and the suspension was stirred under hydrogen at normal pressure and room temperature for 2 hours. The reaction mixture was filtered through siliceous earth and the filtrate was evaporated. There was obtained 0.85 g (95%) of methyl 4-[7-(dimethylamino)heptyl]benzoate as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137920 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-b280573c05484f0a98e7f1a6eb614c14 |
| Source note | uspto-grants-1992_08 |