HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → 2,4-Bis-(acetoxymethyl)-1,5-diisopropylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 1,5-Bis(chloromethyl)-2,4-di(propan-2-yl)benzene | HCID 14850543 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2,4-Bis-(acetoxymethyl)-1,5-diisopropylbenzene | HCID 14850544 | — |
Reaction Steps
40.0 g (154 mmol) of the compound from Example 1 and 22.7 g (277 mmol) of sodium acetate are heated overnight at 80° C. in 200 ml of dimethylformamide. After distilling off the solvent, the residue is taken up with petroleum ether, washed with water and dried using sodium sulphate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05138090 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-09ea600d566a4422a9581aac17eb5544 |
| Source note | uspto-grants-1992_08 |