HRID846878

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID517045

Sodium Acetate

C2H3NaO2

HCID14850543

1,5-Bis(chloromethyl)-2,4-di(propan-2-yl)benzene

C14H20Cl2

PRODUCTS

产物

反应SMILES：CC(=O)OCc1cc(COC(C)=O)c(C(C)C)cc1C(C)C

HCID14850544

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

Dimethylformamide

C3H7NO

PROCEDURE

实验过程

40.0 g (154 mmol) of the compound from Example 1 and 22.7 g (277 mmol) of sodium acetate are heated overnight at 80° C. in 200 ml of dimethylformamide. After distilling off the solvent, the residue is taken up with petroleum ether, washed with water and dried using sodium sulphate.

WORKUP

后处理

distillationAfter distilling off the solvent
washwashed with water
customdried