HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → (4,6-Diisopropyl-1,3-phenylene)dimethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2,4-Bis-(acetoxymethyl)-1,5-diisopropylbenzene | HCID 14850544 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (4,6-Diisopropyl-1,3-phenylene)dimethanol | HCID 14850545 | — |
Reaction Steps
40.2 g (131 mmol) of the compound from Example 2 are stirred at 50° C. for 3 h with 16.1 g (0.3 mol) of potassium hydroxide in 200 ml of methanol. After distilling off the solvent, the residue is taken up in ether, washed with water, dried using sodium sulphate and recrystallized from ethyl acetate/petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05138090 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-df88671860084510912e9327b15a7a7a |
| Source note | uspto-grants-1992_08 |