HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydroxymethyl-4-methoxymethyl-1,5-diisopropylbenzene → 2,4-Diisopropyl-5-ethoxymethyl-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydroxymethyl-4-methoxymethyl-1,5-diisopropylbenzene | HCID 14850546 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,4-Diisopropyl-5-ethoxymethyl-benzaldehyde | HCID 19884344 | — |
Reaction Steps
17.2 g (80 mmol) of pyridinium chlorochromate are added to a solution of 15.7 g (66.5 mmol) of the compound from Example 4 in 300 ml of methylene chloride, the mixture is stirred overnight at room temperature, filtered with suction through kieselgur, washed with 200 ml of methylene chloride, and dried using sodium sulphate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05138090 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-bf5e4e558fd54aa5b737a0ce9623c346 |
| Source note | uspto-grants-1992_08 |