HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide → 2-Tert-butyoxycarbonylamino-3-octadecylcarbonyloxypropylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | 2-Methylcarbamoyloxy-3-octadecylcarbamoyloxypropylamine | HCID 14834999 | — |
| Reactant | 3-Hexadecylthio-2-methoxypropylamine | HCID 14992265 | — |
| Reactant | 2-tert-Butoxycarbonylamino-3-octadecylcarbamoyloxypropane | HCID 19884226 | — |
| Product | 2-Tert-butyoxycarbonylamino-3-octadecylcarbonyloxypropylamine | HCID 131717490 | — |
Reaction Steps
2-tert-Butoxycarbonylamino-3-octadecylcarbamoyloxypropane V e2 is allowed to react and worked up by the same procedure as described in (3). The phthalimide compound: m.p. 127°-129° C., The amino compound IV e2 69°-70° C. The summary of the experimental condition and the physical data of the product are listed in Tables 5 and 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05138067 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-73ae356a95f04ec99243e7972d7dbca4 |
| Source note | uspto-grants-1992_08 |