Phthalimide → 3-Hexadecylthio-2-(3-isoxazolyloxy)propylamine

HRID 846994Notes

Reaction equation

HRID 846994 reaction equation
[CH2:1]([S:17][CH2:18][CH:19]([O:22][C:23]1[CH:27]=[CH:26][O:25][N:24]=1)[CH2:20]O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].C(SCC(OC)C[NH2:48])CCCCCCCCCCCCCCC.C1(=O)NC(=O)C2=CC=CC=C12>>[CH2:1]([S:17][CH2:18][CH:19]([O:22][C:23]1[CH:27]=[CH:26][O:25][N:24]=1)[CH2:20][NH2:48])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 3

HCID 6809PhthalimideHCID 148349913-Hexadecylthio-2-(3-isoxazolyloxy)propanolHCID 149922653-Hexadecylthio-2-methoxypropylamine

Product 1

HCID 148350083-Hexadecylthio-2-(3-isoxazolyloxy)propylamine

Procedure

3-Hexadecylthio-2-(3-isoxazolyloxy)propanol V j1 is allowed to react and worked up by the same procedure as described in (3). The phthalimide compound: m.p. 73°-74° C. The summary of the experimental condition and the physical data of the product are listed in Tables 5 and 6.

Workup

  1. customto react

Sources & evidence

ORD record
ord-c3bbdad32bb749648d79ec282e2c0ff6
Source dataset
uspto-grants-1992_08
Patent number
US05138067

Reaction notes

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