HRID847123

反应详情

EQUATION

反应方程式

HRID 847123 的结构方程式

PROCEDURE

实验过程

Filling in a dry 250 ml flask respectively 57.42 g (0.276 mol) of para-t-butylphenoxyacetic acid synthesized in Example 17 and 80.5 ml of thionyl chloride, the reaction mixture was heated and refluxed for 5-6 hours.

WORKUP

后处理

  1. temperaturerefluxed for 5-6 hours