HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Tert-butylphenoxy)acetic acid → 4-tert-Butylphenoxyacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Tert-butylphenoxy)acetic acid | HCID 15718 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 4-tert-Butylphenoxyacetyl chloride | HCID 611195 | — |
Reaction Steps
Filling in a dry 250 ml flask respectively 57.42 g (0.276 mol) of para-t-butylphenoxyacetic acid synthesized in Example 17 and 80.5 ml of thionyl chloride, the reaction mixture was heated and refluxed for 5-6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05139564 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-b8383f0a2ee648a49bd2fc6b75370584 |
| Source note | uspto-grants-1992_08 |