HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 19882341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 12497321 | HCID 12497321 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19882341 | HCID 19882341 | — |
Reaction Steps
A mixture of 4-(4-nitrophenylthio)-1-butanol (10 mmol) and potassium carbonate (20 mmol) in acetone (100 mL) is treated with a solution of benzylbromide (11 mmol) in acetone (50 mL). When the addition is completed the mixture is heated at reflux temperature for 18 hrs, cooled, filtered, and the filtrate is concentrated to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140026 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-3c52e80894a645969fb1530aa7f0e9f3 |
| Source note | uspto-grants-1992_08 |