HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19882346, compound → HCID 19882368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19882346 | HCID 19882346 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19882368 | HCID 19882368 | — |
Reaction Steps
A solution of N-[2-(4-morpholinyl)ethyl]-S-(4-nitrophenyl)-S-[4-(phenylmethoxy)butyl]sulfoximine in ethanol is treated under nitrogen with 5% palladium on carbon catalyst and the mixture is subjected to catalytic hydrogenation on a Parr apparatus at 70° C. When hydrogen uptake ceases, the catalyst is removed by filtration and the filtrate concentrated to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140026 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-1ace1d09facf459589c06ee38ebc7611 |
| Source note | uspto-grants-1992_08 |